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X-ray Structure Determination: A Practical Guide

X-ray Structure Determination: A Practical Guide

ISBN 9780471607113
Edition 2 Rev ed
Publication Date
Publisher John Wiley and Sons Ltd
Closely follows an actual structural determination. After some introductory material on the nature of x--rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x--ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the "phasea a problem, the principal difficulty in x--ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.

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